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Mechanochemical synthesis of tetramic acids and their biomimetic ring expansion to 4-hydroxy-2-pyridones
DOI: 10.1039/D5GC03085D, Communication
Open Access 
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Kalliopi Mazaraki, Aimilia Eirini Tsirozidou, Basil Kakarikas, Alexandros L. ZografosRolling towards pyridones: ball milling enables green tetramic acid synthesis and its smooth biomimetic expansion to valuable heterocycles.
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An in situ phosphorization constructed VP2@VS2 nanoflower heterostructure with a modulated d-band center of V for efficient polysulfide adsorption and conversion in lithium–sulfur batteries
DOI: 10.1039/D5GC03028E, PaperZhidong Ye, Yaxiong He, Huasheng Gao, Heming Hu, Tao Chen, Qi Jiang
Li-S: low cost, high energy (≈2600 Wh kg−1), abundant S. VP2@VS2 enables triple synergy: LiPSs adsorption, d-band optimization, Li2S barrier reduction. 88% retention after 1000 cycles@2C, suppresses shuttle, enables renewable storage.
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NAD(H) self-recycling whole-cell biocatalysis for the production of furoic acid and 2,5-furandicarboxylic acid from furfural via CO2 fixation
DOI: 10.1039/D5GC03156G, CommunicationMingzhe Ma, Yajie Wang
A whole-cell catalytic system facilitates the conversion of furfural to 2,5-furandicarboxylic acid through an NAD(H)-self-sufficient enzyme cascade coupled with CO2 fixation.
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D-band center modulation of Prussian blue analogues through a high-entropy strategy for aqueous potassium-ion batteries
DOI: 10.1039/D5GC03109E, PaperFuping Min, Qi Zhang, Usman Ali, Maoyu Sun, Fayin Liu, Yueqi Xu, Lu Li, Chungang Wang, Bingqiu Liu
On the basis of the d-band center theory, we employed a high-entropy strategy to regulate the d-band center of Fe-based PBAs to enhance the strength of the Fe–CN bond, which exhibits outstanding cycling stability over 10 000 cycles.
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Metal-free triphenyl phosphite-catalyzed Ritter-type amidation of allylic alcohols
DOI: 10.1039/D5GC03351A, PaperLongzhi Zhu, Furong Guo, Weiwei Luo, Shuangjiao Xie, Tingyuan Zhu, Zihe Liao, Biquan Xiong, Yu Liu, Ke-Wen Tang, Renhua Qiu
A triphenyl phosphite-catalyzed, metal-, oxidant- and additive-free Ritter-type amidation of allylic alcohols is described for the first time, enabling precise regiocontrolled synthesis of amides with 100% atom economy under mild conditions.
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A novel carbon-free 3D porous honeycomb-like MoS2/ReS2 heterostructure with S vacancies as anodes for sodium-ion batteries
DOI: 10.1039/D5GC02014J, PaperMinghui Ding, Siyi Chen, Tianyu Xue, Mingyu Xie, Junying Weng, Dongming Liu, Lechen Diao, Pengfei Zhou
A novel carbon-free 3D porous honeycomb-like MoS2/ReS2-S heterostructure with S vacancies was designed and applied as an anode material for sodium-ion batteries, demonstrating excellent electrochemical performance.
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Tracking the hydrogen spillover of heterogeneous catalysts in hydrogenation: from formation, migration, and regulation to fate
DOI: 10.1039/D5GC02983J, Tutorial ReviewGuangxun Sun, Peng Xue, Lei Wang, Xin Zhang, Guangzheng Sun, Zhidong Wang, Qian Zhang, Peng Zhang, Yunqi Liu, Yuan Pan
The review “Tracking the hydrogen spillover of heterogeneous catalysts in hydrogenation: from formation and fate to regulation” discusses the challenges in structure optimization and offers strategies to enhance hydrogen spillover efficiency.
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A bioinspired heterogeneous catalyst for green and targeted transesterification of ethanol and dimethyl carbonate to ethyl methyl carbonate with high endurance
DOI: 10.1039/D5GC03241E, PaperRongkai Cui, Fengyue Yin, Wangquan Gong, Ningjing Yan, Siyao Li, Changshen Ye, Ting Qiu, Jie Chen
Developing an efficient and sustainable method for producing ethyl methyl carbonate (EMC), a key electrolyte component in lithium-ion batteries, is essential to meet the growing industrial demand and comply with green chemistry principles.
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Green epoxidation of unactivated alkenes via the catalytic activation of hydrogen peroxide by 4-hydroxybenzaldehyde
DOI: 10.1039/D5GC02537K, Paper
Open Access   This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Efthymios T. Poursaitidis, Christiana Mantzourani, Ierasia Triandafillidi, Maroula G. Kokotou, Christoforos G. KokotosAn organocatalytic protocol that utilizes 4-hydroxybenzaldehyde as an activator of H2O2 for the epoxidation of unactivated olefins is described. An unprecedented Payne/Dakin tandem mechanistic scenario is presented, supported by DI-HRMS experiments.
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Interfacial molecular engineering-driven self-emulsification: a green strategy for surfactant-free, high-efficiency oral delivery of cyclosporine A
DOI: 10.1039/D5GC02056E, PaperPeiya Shen, Enshi Hu, Jitong Shi, Ruipeng Li, Xingyu Zhu, Yuan Gao, Jianjun Zhang, Yuanfeng Wei, Shuai Qian
A green chemistry strategy for oral peptide delivery using biodegradable cellulose and food-grade trans-anethole enables solvent-free self-emulsification, enhancing bioavailability while minimizing environmental impact and energy use.
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Engineered Pseudomonas putida monoculture system for green synthesis of 7-methylxanthine
DOI: 10.1039/D5GC02883C, PaperBhagya Jayantha, Shuyuan Zhang, Ryan M. Summers, Gamini P. Mendis, Lahiru N. Jayakody
Engineered Pseudomonas putida monoculture efficiently converts caffeine to 7-methylexanthine (7-MX), a clinically proven safe drug for treating myopia.
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Lignin refinement based on efficient thermo-photo-catalysis of Ru–RuO2/TiO2-deep eutectic solvents
DOI: 10.1039/D5GC02098K, PaperHekun Ding, Yue Pan, Ao Zhan, Jie Lv, Yang Yang, Zhiyuan Yang, James H. Clark, Qiang Yu
A highly effective thermo-photo-catalysis system was developed combining deep eutectic solvents (DESs) and a Ru–RuO2/TiO2 composite to enable efficient catalytic depolymerization of lignin into phenol under clean and mild conditions.
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Plasmon-driven enhancement in CO2 photoreduction: Mechanistic elucidation and materials design strategies
DOI: 10.1039/D5GC03066H, Tutorial ReviewHouxu Zhou, Suwei Wang, Pin Song, Yi Zhang, Wei Jiang, Jun Di
The review highlights plasmon materials' advancements in CO2 photoreduction. These materials enhance both light utilization and reaction kinetics via localized electromagnetic fields, hot electron injection, and photothermal synergy.
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Electroenzymatic cascade synthesis of 2,3-diaminophenazine on HRP-ZnGa2O4 nano-biohybrids
DOI: 10.1039/D5GC03726C, PaperYuxuan Cheng, Zhe Wang, Siqi Li, Meixuan Li, Shuni Li, Xue Xiao, Yucheng Jiang, Yu Chen
In this work, a novel nano-biohybrid has been developed for the efficient synthesis of 2,3-diaminophenazine (DAP), a biologically significant heterocyclic compound, via an electroenzymatic cascade catalysis system.
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Advancing lignocellulosic conversion though biosensor-enabled metabolic engineering
DOI: 10.1039/D5GC03618F, Tutorial Review
Open Access 
  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Qi Gan, Jianli Zhang, Xinyu Gong, Yusong Zou, Yajun YanBiosensor-aided metabolic engineering is advancing the conversion of lignocellulosic biomass by enabling regulation and optimization of microbial production pathways.
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Improved rare earth element recycling using a sustainable diglycolamide-based hydrophobic eutectic solvent
DOI: 10.1039/D5GC01707F, Paper
Open Access   This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.B. Bernicot, G. Arrachart, S. Dourdain, N. Schaeffer, A. C. Dias, S. Pellet-RostaingA hydrophobic eutectic solvent is shown to efficiently recover rare earth elements from waste leachates with a lower environmental impact than the comparable traditional solvent extraction system.
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Photoinduced carbonylative multicomponent reaction of anilines and arylaldehydes
DOI: 10.1039/D5GC02973B, Communication
Open Access   This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Mao-Lin Yang, Xiao-Feng WuA photoinduced carbonylative amination strategy with arylaldehydes, enabling the efficient synthesis of valuable α-aminoketones has been developed.
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Phosphatidylcholine-driven cell-like assembly of lignin for reinforcing and toughening rubber materials
DOI: 10.1039/D5GC01947H, PaperJunqi Zhang, Jianlong Wen, Zhenwei Liu, Fangwei Ling, Zhengtian Xie, Yijing Nie, Jinrong Wu
This work employs phosphatidylcholine to modulate the polarity of lignin, enabling lignin to form a self-assembled ‘cell-like structure’ within HPIP. The resulting composites achieve a remarkable strength of 26 MPa while maintaining excellent recycling capability.
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Toward closed-loop hydrometallurgy: a critical review of wastewater reuse strategies for end-of-life LiFePO4 battery recycling
DOI: 10.1039/D5GC02987B, Critical ReviewJong-Won Choi, Hyun-Woo Shim, Hong-In Kim, Sookyung Kim, Duy Tho Tran, Mooki Bae
A closed-loop hydrometallurgical route incorporating wastewater reuse for sustainable recycling of low-value LFP batteries.
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Microwave-assisted pyrolysis of biomass and plastic wastes for hydrogen production
DOI: 10.1039/D5GC03030G, Critical ReviewYafei Shen
This review summarizes the recent advances and future challenges in the microwave-intensified pyrolysis of biomass and plastic wastes for H2 production.
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